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49th
Annual (2000) DXC > Monday Workshops (July 31)
a.m. workshops: 9:00a.m.-12 noon p.m.
workshops: 2:00p.m.-5:00 p.m.
(unless otherwise noted)
Morning Workshops: XRF & XRD(W-1) - XRD(W-2
& W-3) - XRF(W-4)
Evening Workshops: XRD(W-5
& W-6) - XRF(W-7 & W-8)
Workshops, Monday a.m.
XRD & XRF
W-1
New Methods of Beam Conditioning (Evergreen A)
| Organizer: |
J. Faber |
International
Centre for Diffraction Data, Newtown Square, PA |
| Instructors: |
J. Faber |
International
Centre for Diffraction Data, Newtown Square, PA |
|
D.K. Bowen |
Bede
Scientific, Inc., Englewood, CO |
This workshop discusses traditional and newer methods of X-ray
beam conditioning, as applied to both X-ray diffraction and X-ray fluorescence.
XRD
W-2
Hands on Rietveld Analysis I (Bring
your own computer) (Evergreen
B)
| Organizers: |
R.E. Dinnebier |
University
of Bayreuth, Bayreuth, Germany |
|
E. Antipov |
Moscow
State University, Moscow, Russia |
| Instructors: |
R.E. Dinnebier |
University
of Bayreuth, Bayreuth, Germany |
|
E. Antipov |
Moscow
State University, Moscow, Russia |
|
R. VonDreele |
Los
Alamos National Laboratory, Los Alamos, New Mexico |
|
P.W. Stephens |
State
University of New York at Stony Brook, Stony Bro |
The Rietveld method is a fast-developing technique. This course
is intended for beginners as well as advanced users and will cover many new features such as: advanced
peak profile functions, rigid bodies with satellite groups, planarity restraints, modeling of
anisotropic half-widths due to lattice strain, etc. After the lectures, all participants will have the opportunity to
practice* using the well known "GSAS" program system. A well-prepared example exhibiting different
levels of complexity will be provided. Participants are also welcome to bring their own datasets.
*In order to participate hands-on, you must bring your own laptop
computer and load the appropriate software, prior to attending the workshop. Please visit the web page
http://www.pulverdiffraktometrie.de/Education/rietveld/rietveld.html
for detailed instructions on how to obtain the necessary software.
W-3
Alignment & Standards (Evergreen C)
| Organizers &
Instructors: |
J.P. Cline |
National
Institute of Standards & Technology, Gaithersburg, MD |
|
R.W. Cheary |
University
of Technology Sydney, New South Wales, Australia |
This workshop will discuss NIST Standard Reference Materials, the
basic design of the conventional diffractometer, and how to realize optimal diffractometer performance through
proper alignment and selection of optical components (eg., divergence slits, Soller slits,
etc.). Various alignment procedures will be discussed with consideration given to the consequences of
misalignment and missetting of the components. nstrument calibration and performance will be evaluated through
the use of NIST Standards and the simulation of line profiles.
XRF
W-4
Practical TXRF (Evergreen D)
| Organizer: |
M.A. Zaitz |
IBM
Microelectronics, Hopewell Junction, NY |
| Instructors: |
M.A. Zaitz |
IBM
Microelectronics, Hopewell Junction, NY |
|
P. Wobrauschek |
Atominstitut
der Österreichischen Universitäten, Vienna, Austria |
|
C. Streli |
Atominstitut
der Österreichischen Universitäten, Vienna, Austria |
This workshop will cover the basics of total reflection X-ray
fluorescence, as well as instrumentation, calibration, and applications
Workshops, Monday p.m.
XRD
W-5
Hands on Rietveld Analysis II (Bring
your own computer) (Evergreen
B)
| Organizer: |
R.E. Dinnebier |
University of
Bayreuth, Bayreuth, Germany |
|
E. Antipov |
Moscow
State University, Moscow, Russia |
| Instructors: |
R.E. Dinnebier |
University of
Bayreuth, Bayreuth, Germany |
|
E. Antipov |
Moscow
State University, Moscow, Russia |
|
R. VonDreele |
Los
Alamos National Laboratory, Los Alamos, New Mexico |
|
P.W. Stephens |
State
University of New York at Stony Brook, Stony Brook, NY |
Continuation of W-2.
*In order to participate hands-on, you must bring your own laptop
computer and load the appropriate software, prior to attending the workshop. Please visit the web page
http://www.pulverdiffraktometrie.de/Education/rietveld/rietveld.html
for detailed instructions on how to obtain the necessary
software.
W-6
Analysis of Micron Size Specimens (Evergreen A)
| Organizer: |
R. Goehner |
Sandia
National Laboratories, Albuquerque, NM |
| Instructors: |
R. Goehner |
Sandia
National Laboratories, Albuquerque, NM |
|
R. Tissot |
Sandia
National Laboratories, Albuquerque, NM |
|
G. Ice |
Oak Ridge
National Laboratory, Oak Ridge, TN |
|
P.-C. Wang |
IBM
Corporation Microelectronics Division, Hopewell Junction, NY |
The workshop will describe methods and techniques used to analyze
micron size specimens. Instructors will cover such topics as the use of Scanning
Electron Microscopy for crystallographic evaluation, synchrotron based X-ray microbeam characterization of
thin films in very-large-scale-integrated circuits, recent advances in synchrotron based 3-D X-ray crystal
microscopes, and the use of laboratory-based X-ray sources and 2-D area detectors for
small specimen analysis. Please bring your questions and ideas to this open forum workshop.
XRF
W-7
An Introduction to X-ray Fluorescence (Evergreen C)
| Organizer: |
R. Jenkins |
International
Centre for Diffraction Data, Newtown Square, PA |
| Instructors: |
R. Jenkins |
International
Centre for Diffraction Data, Newtown Square, PA |
|
J. Croke |
Philips
Analytical, Inc. (retired), Mahwah, NJ |
This workshop is intended for beginners and those fairly new to
the field of X-ray fluorescence analysis. The principles behind the technique, along with a description of
the basics, of X-ray spectra and absorption effects will be introduced. The various types of
instrumentation used in the field, including a "compare and contrast" of the features of wavelength
and energy dispersive spectrometers, will also be presented. The use of both techniques for qualitative
analysis will be covered. Additionally, brief coverage on specimen preparation methods an introduction to
the basic concepts behind quantitative analysis will be offered.
W-8
Analysis of Layered Materials by XRF (Evergreen D)
| Organizer: |
M.W. Dirken |
Philips
Analytical, Almelo, The Netherlands |
| Instructors: |
M.W. Dirken |
Philips
Analytical, Almelo, The Netherlands |
|
M. Mantler |
Vienna
University of Technology, Vienna, Austria |
|
A. Wittkopp |
Rontgenanalytik,
Taunusstein-Neuhof, Germany |
This workshop provides an introduction to the analysis of layered
materials, and is intended for the X-ray spectroscopist who encounters this analysis for the first
time. Therefore, the physics and various analysis models are presented. This is followed by contributions
on ED-XRF and WD-XRF examples, focusing on practical issues including problems of finite
thickness and line selection.
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